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Both β-FeSi 2 and β-Fe 0.95 Co 0.05 Si 2 samples were crushed in an agate mortar and milled in a Fritsch "Pulverisette 7" planetary micromill (Fritsch, Idar-oberstein, Germany). A silicon nitride container of 45 mL and five 15 mm-diameter balls were used as the milling media with a ball-to-powder mass ratio set to 10:1.

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The thickness of the GDC layer was reduced to 1.95 µm and the cross-sectional densification was greatly improved with less porosity. In the side view of the half-cell (Fig. 10(c)), the warpage of the sintered half-cell was alleviated to be comparable to the pre-adjustment after sintering. The flatness of the half-cell substrate was improved to ...

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Herein, we develop a protocol for the synthesis of polyimides in high yields and short reaction times of usually less than 1 h (Figure 1 ). As a model reaction the polymerization between pyromellitic dianhydride (PMDA) and 1,3,5-tri (4-aminophenyl)benzene (TAB) was chosen. Furthermore, we expanded the concept to different polymer architectures.

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Sample paths were drawn in the micromill software as either points or lines at 0.5 to 1.0 mm intervals and then computer milled to a depth of 0.5 to 1.0 mm ( Fig. 3 B).

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The "pulverisette 7" planetary micromill is universally applicable for quick dry or wet grinding of inorganic and organic samples for analysis, quality control, materials testing and mechanical alloy-ing. In synthesis, the planetary micromill can be used for mixing and homogenisation of dry samples, of emulsions and of pastes.

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